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  • 2023

    10-31

    氣相色譜儀以其分離效率高、靈敏、快速等優(yōu)點而被各行各業(yè)廣泛應(yīng)用。隨著氣相色譜儀的普及,操作人員如何正確使用儀器,成了一個不可忽視的問題。1、環(huán)境條件國產(chǎn)氣相色譜儀對環(huán)境溫度要求并不苛刻,一般在5~35℃的室溫條件下即可正常操作。但對于環(huán)境濕度一般要求在20%~85%為宜。在高度潮濕的地區(qū),使用某些型號儀器的氫火焰離子化檢測器時,會因濕度大,而導(dǎo)致放大器絕緣性能下降,若在高靈敏度擋上操作,響應(yīng)值會下降。分析人員在使用儀器時,若遇到上述現(xiàn)象,應(yīng)采取必要的措施。2、氣體純度國產(chǎn)氣相...

  • 2023

    10-31

    熱裂解氣相色譜儀分析原理熱裂解氣相色譜法是在一定的條件下高分子及非揮發(fā)性有機物遵循一定的規(guī)律裂解,即特定的樣品能夠產(chǎn)生特征的裂解產(chǎn)物及產(chǎn)物分布,據(jù)此可對原樣品進行表征。把待測樣品置于熱裂解器中,在嚴格控制條件下快速加熱,使之快速分解稱為可揮發(fā)性的小分子產(chǎn)物,然后將裂解產(chǎn)物送入氣相色譜儀毛細管色譜柱中分離,通過對裂解產(chǎn)物的定性和定量分析以及和裂解溫度、裂解時間等操作條件的關(guān)系,可以研究裂解產(chǎn)物和原樣品組成、結(jié)構(gòu)和物化性能關(guān)系,并可以研究裂解機理和反應(yīng)動力學(xué)。PYGC(PX-10...

  • 2023

    10-21

    X熒光光譜儀測試方法:1、X熒光光譜儀樣品制備進行x射線熒光光譜分析的樣品,可以是固態(tài),也可以是水溶液。無論什么樣品,樣品制備的情況對測定誤差影響很大。對金屬樣品要注意成份偏析產(chǎn)生的誤籌;化學(xué)組成相同,熱處理過程不同的樣品,得到的計數(shù)率也不同;成份不均勻的金屬試樣要重熔,快速冷卻后車成圓片;對表面不平的樣品要打磨拋光;對于粉末樣品,要研磨至300目一400目,然后壓成圓片,也可以放人樣品槽中測定。對于固體樣品如果不能得到均勻平整的表面,則可以把試樣用酸溶解,再沉淀成鹽類進行測...

  • 2023

    10-21

    作為歐盟立法制定相對嚴格的健康產(chǎn)品標準的一項強制性標準,ROHS檢測儀是絕大多數(shù)企業(yè)所需求的,生活中的任何事物都有可能與它息息相關(guān),然而人們是怎么通過ROHS檢測儀器發(fā)現(xiàn)它的呢?ROHS檢測儀就是X射線熒光光譜儀,其分析事理也就是X射線熒光光譜儀的分析事理。X射線熒光光譜儀常日可分為兩大類,波長色散X射線熒光光譜儀(WDXRF)和能量色散X射線熒光光譜儀(EDXRF),波長色散光譜儀緊張部件包括激發(fā)源、分光晶體和測角儀、探測器等,而能量色散光譜儀則只需激發(fā)源和探測器和干系電子...

  • 2023

    10-12

    全氟辛基磺酸及其鹽類和全氟辛基磺酰氟(簡稱PFOS)由于同時具備疏油、疏水等特性,被廣泛用于生產(chǎn)紡織品、皮革制品、家具和地毯等表面防污處理劑。全氟辛酸及其鹽類和相關(guān)化合物(簡稱PFOA)主要應(yīng)用包括家用產(chǎn)品表面處理(如不沾鍋炊具)方便食品包裝等。上述兩大類產(chǎn)品由于具有持久性、生物累積性和毒性,都已分別進入了斯德哥爾摩公約,因此在全球范圍內(nèi)受到嚴格管理,除了特定豁免用途或特定用途外,逐步在市場上被淘汰。以下將重點分析這兩大物質(zhì)在歐洲,美國和中國的管理情況。歐洲:在歐洲,有單獨的...

  • 2023

    10-12

    關(guān)于RoHSRoHS指令限制物質(zhì)的種類RoHS指令于2003年2月13日在15個EU(歐盟)國家生效。EC成員國于2006年開始實施,6種物質(zhì)在此處受到監(jiān)管。之后,2015年又增加了4種物質(zhì),現(xiàn)在共有10種物質(zhì)受到管制。在這里,我們將解釋每種材料的概要和特性。RoHS指令要求分析的6種管制物質(zhì)首先,我想解釋一下自2006年7月1日起受到管制的6種物質(zhì)各自的特點。1.鉛(Pb)可以預(yù)期通過增加含量來提高可加工性的鉛。但是,它也以毒性著稱,有人指出,如果攝入過多會導(dǎo)致“鉛中毒”。...

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新典儀器(杭州)有限公司 公司地址:杭州市濱江區(qū)長河街道聚才路105號1號樓301室   技術(shù)支持:化工儀器網(wǎng)
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